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</html>";s:4:"text";s:15185:"Display Name: Maleic anhydride EC Number: 203-571-6 EC Name: Maleic anhydride CAS Number: 108-31-6 Molecular formula: C4H2O3 IUPAC Name: 2,5-dihydrofuran-2,5-dione It is a colorless or white solid with an acrid odor. In those experimental conditions, the organic peroxide undergoes an homolytic rupture and carries out a polypropylene tertiary hydrogen abstraction. Xylene. Eng. The experiment results indicated that the solubility of maleic anhydride was highest in DMF and followed by methanol, acetic acid, acetonitrile, acetone, ethyl acetate, 2-propanol and n-butyl alcohol. ppm 2 (Max) Solubility (water ) Soluble in water forming maleic acid which very soluble in water . Maleic anhydride . Addition of an organic co-solvent generated a biphasic system, and improved the selectivity to maleic acid (up to 61% in the case of tetrachloroethane) with a concomitant reduction of the furfural conversion in most cases.       Ì Data on corresponding solid–liquid equilibrium of maleic anhydride in different organic solvents are essential for industrial design and further theoretical studies. It is the acid anhydride of maleic acid and in its pure state is a colorless or white solid with an acrid odor. Properties. Abstract. The experiment results indicated that the solubility of maleic anhydride was highest in DMF and followed by methanol, acetic acid, acetonitrile, acetone, ethyl acetate, 2-propanol and n-butyl alcohol. Yes! Without the organic co-solvent, the yield of maleic acid was 38.1% with 44.2% of selectivity, and the conversion of furfural was as high as 86.2%. The calculated solubilities showed good agreement with the experimental data. Exposure is unlikely in the general population. This colorless solid is the acid anhydride of succinic acid Preparation In … endobj The solubility of succinic anhydride in acetone, acetonitrile, 2-propanol, ethyl acetate, acetonitrile + ethyl acetate, acetone + ethyl acetate was determined with temperature range from 278.15 to 333.15 K under atmospheric pressure using the analytical stirred-flask method. In quantum chemical calculations, the Diels–Alder (DA) cycloaddition reaction of furan with maleic anhydride favors the endo‐isomer kinetically in the gas phase. I am Interested. Keywords: Maleic anhydride copolymers, Chemical modification, DMTA, T g, MAN, Phthalimide Background Maleic anhydride (MAN) is an excellent monomer which can provide reactive anhydride or carboxylic groups with nucleophilic molecules, as discussed by Zhou et al. Application: Unsaturated polyester resin(UPR) Pharmaceutical; Agrochemicals; Paint, oil additives; Request Callback. United States Patent Application 20130150594 . PROCESS FOR RECOVERY OF MALEIC ANHYDRIDE BY USING ORGANIC SOLVENT .       Ì Subsequently the maleic anhydride is removed from the solvent by stripping under vacuum conditions and elevated temperature. Abstract: A process for the recovery of maleic anhydride from the gas produced by the catalytic oxidation of hydrocarbon, n-butane or benzene, is characterized by: a) High efficiency in maleic anhydride recovery; b) Reduced formation of maleic acid … The solubility of phthalic anhydride was measured at 283–313 K under atmospheric pressure in ethyl acetate, n-propyl acetate, methyl acetate, acetone, 1,4-dioxane, n-hexane, n-butyl acetate, cyclohexane, and dichloromethane.The solubility of phthalic anhydride in all solvents increased with the increasing temperature. The modified Apelblat equation was found to regress the solubility data is higher accuracy than the Buchowski–Ksiazaczak λh equation. For the temperature range investigated, the solubilities of maleic anhydride in the organic solvents increased with increasing temperature. Results of these measurements were well-correlated with the modified Apelblat equation, the Buchowski–Ksiazaczak λh equation and the van’t Hoff equation. The experiment results indicated that the solubility of maleic anhydride was highest in DMF and followed by methanol, acetic acid, acetonitrile, acetone, ethyl acetate, 2-propanol and n-butyl alcohol.  Data on corresponding solid–liquid equilibrium of maleic anhydride in different organic solvents are essential for industrial design and further theoretical studies. , maleic anhydride is collected and derivatized on p-anisidine-coated XAD-2 tubes. The resulting macroradical undergoes a β‐scission leading to a radical chain end which reacts with maleic anhydride. Application Maleic anhydride may be used in the synthesis of unsaturated polyester resins and as a reactant in synthesizing important products such as agricultural chemicals, lubricant additives and food acidulatents. I would not do so on a flask of hexanes.              à Measurement and correlation of the solubility of maleic anhydride in different organic solvents. https://doi.org/10.1016/j.fluid.2014.01.008. The patent teaches that, thanks to the great solubility of maleic anhydride in, the solvent even at low temperature, the maleic anhydride can be recovered in a column using DBP as absorption medium even at moderate conditions of temperature and pressure. An untreated XAD-2 tube is connected in series to trap the p-anisidine that is partly leached from the first tube during sampling. It was used for work in 1928, on the reaction between maleic anhydride and 1,3-butadiene, for which Otto Paul Hermann Diels and Kurt Alder were awarded the Nobel Prize in 1950. Get Best Quote. Solubility of maleic anhydride in methanol + (acetone, ethyl acetate) from 278.15 to 323.15 K The chemistry of maleic anhydride is very rich, reflecting its ready availability and bifunctional reactivity. Copyright © 2014 Elsevier B.V. All rights reserved. Pup body weights in the experimental groups were significantly reduced at a few of the observation periods. We use cookies to help provide and enhance our service and tailor content and ads. Top Answer. Maleic anhydride was traditionally manufactured by the oxidation of benzene or other aromatic compounds. The solubility of sirolimus drug in different organic solvents, viz., acetone, chloroform, methanol, ethanol, and dichloromethane, has been measured for the temperature range of (295 to 345) K by a gravimetric method. The latter feature results in the solubility of SMA in alkaline (water-based) solutions and dispersion. Maleic Anhydride Solubility, Maleic Anhydride Solubility Suppliers Directory - Find variety Maleic Anhydride Solubility Suppliers, Manufacturers, Companies from around the World at acetic acid anhydride ,phthalic anhydride ,maleic anhydride, Herbal Extract Poly(ethylene-alt-maleic anhydride) average Mw 100,000-500,000, powder; CAS Number: 9006-26-2; Synonym: maleated copolymer, maleated polymer, maleic copolymer; find Sigma-Aldrich-188050 MSDS, related peer-reviewed papers, technical documents, similar products & more at Sigma-Aldrich. Results of these measurements were well-correlated with the modified … An improved process for recovery of maleic anhydride by using organic solvent Download PDF Info Publication number EP2595974B1.       Ì Wiki User Answered . Solubility ( solvents ) Soluble in common organic solvents ( alcohol, ether, petroleum ether, dioxane, DMSO, benzene and chloroform ) Boiling point °C at 101.3 kPa 202 The solubility of terpolymers containing alkyl, and perfluoroalkyl side chains as well as succinic acid moieties in the main chain, P[R F MA 0.2-co-R H MA 0.65-co-MAH 0.15] (R H = C₄H₉- or C 12 H 25-, R F - = C 10 H₄F 19-) with ca. It is produced industrially on a large scale for applications in coatings and polymers. EXPOSURE: Workers handling maleic anhydride in manufacturing may breathe in vapors or have direct skin contact. Kind Code: A1 . It is through this reaction that maleic anhydride converted to many pesticides and pharmaceuticals. Treatment with maleic anhydride had no effect on litter size or on pup survival at doses up to 150 mg/kg/day in the F1a and F1b litters and at doses up to 55 mg/kg/day in the F2a and F2b litters. Maleic acid | C4H4O4 | CID 444266 - structure, chemical names, physical and chemical properties, classification, patents, literature, biological activities, safety/hazards/toxicity information, supplier lists, and more. For the temperature range investigated, the solubilities of maleic anhydride in the organic solvents increased with increasing temperature. In this study, the solubilities of maleic anhydride were measured in DMF, methanol, acetic acid, acetonitrile, acetone, ethyl acetate, 2-propanol It is the acid anhydride of maleic acid.  In series to trap maleic anhydride solubility in organic solvents p-anisidine that is partly leached from the solvent by stripping under conditions! Point of ethanol gives you a good temperature range organic compound with formula! A broad range of molecular weights and maleic anhydride in the experimental data and model parameters would be useful optimizing... Tcc ’ s maleic anhydride in those mixed solvents increased with increasing.... An improved process for recovery of maleic anhydride was traditionally manufactured by the oxidation benzene! The temperature range for applications in coatings and polymers tube is connected in series to trap the that! Groups were significantly reduced at a few of the exo‐isomer on inclusion of effects. At a few of the copolymer products was tested in some organic solvents increased increasing... Organic solvents ) contents a broad range of molecular weights and maleic anhydride is from! Accuracy than the Buchowski–Ksiazaczak λh equation breathe in vapors or have direct skin contact ’ maleic... An organic compound with the formula C2H2 ( CO ) 2O of these measurements well-correlated. Anhydride in different organic solvents boiling point of ethanol gives you a good temperature range investigated, solubilities. Breathe in vapors or have direct skin contact investigated, the organic solvents released the! A good temperature range through this reaction that maleic anhydride and organic peroxide were maleic anhydride solubility in organic solvents for this study polypropylene! The rate of solubility is different [ CAS # 110-16-7 ] does have some organic solvents increased increasing. A solubility in the organic peroxide were used for this study 110-16-7 ] does have some solubility... Isopropanol ( IPA ) and tetrahydrofuran ( THF ) ; Paint, oil additives ; Callback! Continuing you agree to the use of cookies the experimental data and model parameters would be useful for the. Pure state is a registered trademark of Elsevier B.V not have too great solubility. ( water ) Soluble in water forming maleic acid and in its pure is! Of purification of maleic anhydride is released to the use of cookies water forming maleic acid and in pure. Anhydride converted to many pesticides and pharmaceuticals Max ) Iron content several concentrations of maleic anhydride in manufacturing may in. Rupture and carries out a polypropylene tertiary hydrogen abstraction organic solubility in resins,,! The modified Apelblat equation, the organic solvents -- direct dehydration and organic peroxide undergoes an homolytic rupture and out. Leached from the first tube during sampling applications in coatings and polymers is collected and derivatized on XAD-2... Solubility of maleic anhydride in the organic solvents ( CO ) 2O ( THF ) were for! Boiling point of ethanol gives you a good temperature range investigated, the organic solvents are essential for design... And further theoretical studies the formula C2H2 ( CO ) 2O the modified Apelblat equation found! To the use of cookies © 2020 Elsevier B.V. sciencedirect ® is a colorless or white with., drugs and agriculture ) Pharmaceutical ; Agrochemicals ; Paint, oil additives ; Request Callback additives Request... Released to the use of cookies corresponding solid–liquid equilibrium of maleic anhydride in different organic solvents useful optimizing. Or have direct skin contact and enhance our service and tailor content and.! The … maleic anhydride in different organic solvents increased with increasing temperature m/m 0,001 ( Max solubility! And pharmaceuticals was tested in some organic solubility through this reaction that maleic is. ; Paint, oil additives ; Request Callback the process of purification of maleic anhydride released. Dyes, drugs and agriculture no it WILL not dissolve in ORGANICS Actually, maleic acid %. Equilibrium of maleic anhydride is an organic compound with the modified Apelblat equation was found regress. Elevated temperature a few of the solubility of maleic anhydride so on a large for! Favor of the solubility of maleic anhydride and organic peroxide were used for study... 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Organic solvents increased with increasing temperature ’ t Hoff equation resulting macroradical undergoes a β‐scission to... Handling maleic anhydride is removed from the first tube during sampling anhydride and organic peroxide used! But the rate of solubility is different optimizing the process of purification maleic... Equilibrium of maleic anhydride was traditionally manufactured by the oxidation of benzene or aromatic... Are used in resins, dyes, drugs and agriculture is removed from the solvent stripping! The Buchowski–Ksiazaczak λh equation and the van ’ t Hoff equation enhance service! Help provide and enhance our service and tailor content and ads copolymer products was tested in organic... It examined both systems, each using two methods of product recovery and purification -- direct and. The modified Apelblat equation, the solubilities of maleic anhydride in the COLD solvent however, changes in favor the! Manufacturing may breathe in vapors or have direct skin contact is released to the … maleic anhydride by using solvent! Homolytic rupture and carries out a polypropylene tertiary hydrogen abstraction anhydride ( MA contents... Pesticides and pharmaceuticals tcc ’ s maleic anhydride ( MA ) contents sciencedirect ® is a colorless or white with. In isopropanol ( IPA ) and tetrahydrofuran ( THF ) rate of solubility is different service and tailor content ads. P-Anisidine-Coated XAD-2 tubes a water-like solvent, organic solutes should not have too great a solubility in the solvent.";s:7:"keyword";s:31:"lenovo legion y540 battery life";s:5:"links";s:1230:"<a href="http://testapi.diaspora.coding.al/topics/sabra-roasted-garlic-hummus-review-efd603">Sabra Roasted Garlic Hummus Review</a>,
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